Characterization of cyanide-responsive fluorogenic probes (2024)

Available

Dataset

Licence : CC BY-NC-SA doi:10.25666/DATAUBFC-2024-07-17

Data creators : Anthony Romieu ^[1], Vincent Gaumerd ^[1]

[1] : Institut de Chimie Moléculaire de l'Université de Bourgogne (UMR 6302) (Université de Bourgogne)

Description :

Raw spectroscopic data (IR, NMR, mass spectrometry and UV-visible) and RP-HPLC elution profiles of all compounds described in this study. Raw fluorescence data and RP-HPLC-fluorescence/-MS elution profiles related to fluorogenic activation of probes by cyanide ions.

Disciplines :

chemistry, analytical (chemistry), chemistry, organic (chemistry), chemistry, physical (chemistry)

Keywords :

fluorescence analyses, HPLC chromatography, infrared (IR), mass spectrometry (MS), nuclear magnetic resonance (NMR), UV-visible analyses

General metadata

Data acquisition date : from Oct 2022 ongoing

Data acquisition methods :

Experimental data :
Spectroscopic data were acquired using several scientific instrumentation softwares: Bruker OPUS for IR data, Bruker TopSpin for NMR data, Thermo Scientific Xcalibur for high-resolution mass spectra, and Cary WinUV for UV-visible absorption spectra. On the matter of HPLC and fluorescence data, they were obtained using the following softwares: Thermo Scientific Chromeleon and SAFAS SP2000 respectively. Mass data were converted into .pdf format; UV-visible absorption, HPLC and fluorescence data were converted into .csv, .xls or .xslx format directly readable in Excel. Only the processing of IR and NMR data requires the use of Bruker OPUS and TopSpin softwares respectively (free versions of both softwares are currently available, OPUS Viewer and TopSpin academic version) or MestReNova. HPLC data are readable with a PC but not with a Mac.

Update periodicity : as needed

Language : English (eng)

Formats : application/pdf, application/vnd.ms-excel, application/vnd.openxmlformats-officedocument.spreadsheetml.sheet, chemical/x-bsw, chemical/x-cmbx, chemical/x-cmf, chemical/x-FID, chemical/x-OPUS, chemical/x-spf, text/csv

Audience : Research

Publications :

Fluorogenic detection of cyanide ions in pure aqueous media through intramolecular cross-benzoin reaction: limitations unveiled and possible solutions (à soumettre)

Collection :

Données de thèse

Publisher : dataUBFC - Atelier de la donnée de Bourgogne-Franche-Comté

Label : Pôle Chimie Moléculaire

Projects and funders :

DetectOP_BChE - Détection fluorescente et/ou colorimétrique des organophosphorés à base de butyrylcholinestérase
- ANR-18-CE39-0014 (French National Agency for Research)
Thèse de doctorat en chimie - Vincent Gaumerd
- Contrat doctoral de droit privé (ADEME french agency)
- Direction générale de l'armement - Agence de l'innovation de défense (DGA-AID) (Ministry)

Additional information :

Data collected within the thesis work of Vincent Gaumerd, supervized by Anthony Romieu (University Professor). ICMUB laboratory.

Data

	1 file
		Data-Characterization-cyanide-responsive-fluorogenic-probes.zip Published : 17/07/2024 13:42 Size : 326.46 MB Continued Description : All spectroscopic and analytical data related to characterization and validation of cyanide-responsive fluorogenic probes

1 file